4-Iodo-5-nitro-1,2-dimethoxybenzene

Base Information

Chemical Name:4-Iodo-5-nitro-1,2-dimethoxybenzene
CAS No.:14120-13-9
Molecular Formula:C₈H₈INO₄
Molecular Weight:309.06
Hs Code.:
European Community (EC) Number:621-842-0

Synonyms:4-iodo-5-nitro-1,2-dimethoxybenzene;SCHEMBL14785603;JTESSAIGBDTIRH-UHFFFAOYSA-N;AKOS024338968;1,2-DIMETHOXY-4-IODO-5-NITROBENZENE

Suppliers and Price of 4-Iodo-5-nitro-1,2-dimethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Iodo-5-nitro-1,2-dimethoxybenzene

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:308.94981
Heavy Atom Count:14
Complexity:208

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)[N+](=O)[O-])I)OC

Technology Process of 4-Iodo-5-nitro-1,2-dimethoxybenzene

There total 5 articles about 4-Iodo-5-nitro-1,2-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 110190-08-4
1,2-diiodo-4,5-dimethoxybenzene

: 14120-13-9
4-iodo-5-nitro-1,2-dimethoxybenzene

Guidance literature:: With nitric acid; acetic acid; at 20 - 100 ℃;
DOI:10.1002/anie.201106516

Reference yield: 60.0%

: 4998-07-6
4,5-dimethoxy-2-nitro-benzoic acid

: 14120-13-9
4-iodo-5-nitro-1,2-dimethoxybenzene

Guidance literature:: With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper (I) acetate; silver sulfate; sodium iodide; In dimethyl sulfoxide; at 160 ℃; for 24h; Schlenk technique;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 14120-13-9
4-iodo-5-nitro-1,2-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: glacial acetic acid; iodine chloride

2: glacial acetic acid; nitric acid

With nitric acid; Iodine monochloride; acetic acid;