7-Bromo-1-methyl-1H-indole 97%

Base Information

• Chemical Name: 7-Bromo-1-methyl-1H-indole 97%
• CAS No.: 280752-68-3
• Molecular Formula: C9H8 Br N
• Molecular Weight: 210.073
• Hs Code.: 2933998090
• Mol file: 280752-68-3.mol

Synonyms:7-Bromo-1-methyl-1H-indole;7-Bromo-1-methylindole; N-Methyl-7-bromoindole

Chemical Property of 7-Bromo-1-methyl-1H-indole 97%

Chemical Property:

• Vapor Pressure: 0.002mmHg at 25°C
• Melting Point: 50.5-53°C
• Refractive Index: 1.622
• Boiling Point: 300.878°C at 760 mmHg
• Flash Point: 135.766°C
• Density: 1.472g/cm³

Purity/Quality:

99%, ^*data from raw suppliers

7-Bromo-1-methyl-1H-indole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-Bromo-1-methyl-1H-indole 97%

There total 8 articles about 7-Bromo-1-methyl-1H-indole 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-(1-bromopropenyl)-3-vinyl-1H-pyrrole + methyl iodide (74-88-4) → 7-bromo-1-methylindole (280752-68-3)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

Reference yield: 92.0%

7-bromo-1H-indole (51417-51-7) + methyl iodide (74-88-4) → 7-bromo-1-methylindole (280752-68-3)

Guidance literature:

7-bromo-1H-indole; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 1.75h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol3031389

Reference yield: 76.0%

potassium methanolate (865-33-8) + 7-bromo-N-(4-toluenesulfonyl)-1H-indole (189266-03-3) → 7-bromo-1-methylindole (280752-68-3)

Guidance literature:

In acetonitrile; at 20 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.9b02639

upstream raw materials:

7-bromo-1H-indole

dimethyl sulfate

methyl iodide

2-nitrophenyl bromide

Downstream raw materials:

1-methyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

3-(6-Benzyloxy-1H-indol-3-yl)-4-(1-methyl-1H-indol-7-yl)-pyrrole-2,5-dione

2,4,6-Trimethyl-N-[(S)-1-(1-methyl-1H-indol-7-ylmethyl)propyl]benzenesulfonamide

1-methyl-1H-indole-7-carbonitrile

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 280752-68-3 7-Bromo-1-methyl-1H-indole 97%

Send

Send

Metric Ton KG G Pound L ML

Send

Send