4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Base Information

Chemical Name:4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate
CAS No.:1425794-23-5
Molecular Formula:BF₄*C₁₉H₂₄NS₂
Molecular Weight:417.343
Hs Code.:

Synonyms:4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Suppliers and Price of 4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

There total 6 articles about 4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1425794-21-3
4-(2-(2,4-dimethylphenylthio)phenyl)thiomorpholine

: 420-37-1
trimethoxonium tetrafluoroborate

: 1425794-23-5
4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Guidance literature:: In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 1425794-19-9
2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester

: 1425794-23-5
4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

2.1: triethylamine; dmap / dichloromethane / 0.58 h / 80 °C / Inert atmosphere; Microwave irradiation

2.2: 18 h / 20 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 1.5 h / Inert atmosphere; Reflux

3.2: 0.17 h

4.1: dichloromethane / 4 h / 20 °C

With dmap; dimethylsulfide borane complex; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 615-36-1
2-bromoaniline

: 1425794-23-5
4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 72 h / Reflux

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; potassium tert-butylate / toluene / 21 h / 100 °C

3.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

4.1: triethylamine; dmap / dichloromethane / 0.58 h / 80 °C / Inert atmosphere; Microwave irradiation

4.2: 18 h / 20 °C

5.1: dimethylsulfide borane complex / tetrahydrofuran / 1.5 h / Inert atmosphere; Reflux

5.2: 0.17 h

6.1: dichloromethane / 4 h / 20 °C

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dimethylsulfide borane complex; potassium tert-butylate; triethylamine; trifluoroacetic acid; bis[2-(diphenylphosphino)phenyl] ether; In tetrahydrofuran; dichloromethane; toluene;