2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester

Base Information

• Chemical Name: 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester
• CAS No.: 1425794-19-9
• Molecular Formula: C₁₉H₂₃NO₂S
• Molecular Weight: 329.463
• Mol file: 1425794-19-9.mol

Synonyms:2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester

Chemical Property of 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester

There total 4 articles about 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

2,4-dimethyl-thiophenol (13616-82-5) + o-chlorobenzenecarbamic acid tert-butyl ester (35426-69-8) → 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester (1425794-19-9)

Guidance literature:

With tetrabutylammomium bromide; potassium hydroxide; In water; toluene; at 45 ℃; Concentration;

Reference yield: 91.6%

2,4-dimethyl-thiophenol (13616-82-5) + tert-butyl 2-fluorophenylcarbamate (98968-72-0) → 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester (1425794-19-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 - 85 ℃; for 36h; Temperature;

Reference yield:

2,4-dimethyl-thiophenol (13616-82-5) + 2-bromo-N-(tert-butoxycarbonyl)aniline (78839-75-5) → 2-(2,4-dimethylphenylsulfanyl)phenyl carbamic acid tert-butyl ester (1425794-19-9)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether; In toluene; at 100 ℃; for 21h;

upstream raw materials:

di-tert-butyl dicarbonate

2-bromoaniline

2,4-dimethyl-thiophenol

2-bromo-N-(tert-butoxycarbonyl)aniline

Downstream raw materials:

2-(2,4-dimethylphenylsulphanyl)benzeneamine

4-(2-(2,4-dimethylphenylthio)phenyl)thiomorpholine-3,5-dione

4-(2-(2,4-dimethylphenylthio)phenyl)thiomorpholine

4-(2-(2,4-dimethylphenylthio)phenyl)-1-methylthiomorpholin-1-ium tetrafluoroborate