ethylene glycol di-tertbutylphenoxide

Base Information

• Chemical Name: ethylene glycol di-tertbutylphenoxide
• CAS No.: 113487-25-5
• Molecular Formula: C₂₂H₃₀O₂
• Molecular Weight: 326.479
• Mol file: 113487-25-5.mol

Synonyms:ethylene glycol di-tertbutylphenoxide

Chemical Property of ethylene glycol di-tertbutylphenoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethylene glycol di-tertbutylphenoxide

There total 5 articles about ethylene glycol di-tertbutylphenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

para-tert-butylphenol (98-54-4) + 2-chloroethyl tosylate (80-41-1) → ethylene glycol di-tertbutylphenoxide (113487-25-5)

Guidance literature:

para-tert-butylphenol; 2-chloroethyl tosylate; With potassium carbonate; In acetonitrile; for 18h; Heating;

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Further stages.;

DOI:10.1039/b008603g

Reference yield: 21.0%

para-tert-butylphenol (98-54-4) + ethylene dibromide (106-93-4) → ethylene glycol di-tertbutylphenoxide (113487-25-5)

Guidance literature:

With potassium hydroxide; In ethanol; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c8dt02498g

Reference yield:

2-hydroxyethyl 4-methylbenzenesulfonate (42772-85-0) + sodium 4-tert-butylphenolate (5787-50-8) → 2-(4-tert-butyl-phenoxy)-ethanol (713-46-2) + ethylene glycol di-tertbutylphenoxide (113487-25-5)

Guidance literature:

In 1,4-dioxane; toluene; for 3h; Inert atmosphere; Reflux;

DOI:10.1016/j.polymer.2011.07.010

upstream raw materials:

para-tert-butylphenol

1,2-dichloro-ethane

1,2-bis-tosyloxyethane

2-chloroethyl tosylate

Downstream raw materials:

1,2-Bis(4-t-butyl-2-chlorosulfonylphenoxy)ethane

2,2′-[ethane-1,2-diylbis(oxy)]di(5-tert-butyl)benzaldehyde

1,2-bis[2'-(2''-chloroethoxy)-4'-tert-butylphenoxy]ethane

1,2-bis(2'-formyloxy-4'-tert-butylphenoxy)ethane