3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

Base Information

Chemical Name:3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol
CAS No.:219744-39-5
Molecular Formula:C₃₈H₄₆O₇
Molecular Weight:614.779
Hs Code.:

Synonyms:3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

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Chemical Property of 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

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Technology Process of 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

There total 5 articles about 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 219744-38-4
3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propene

: 219744-39-5
3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

Guidance literature:: 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propene; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 0 ℃; for 2h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/ja001903v

Reference yield:

: 6972-79-8
dibenzyl glycerol

: 219744-39-5
3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / NaH / tetrahydrofuran / 20 - 65 °C

2.1: 9-BBN / tetrahydrofuran / 2 h / 0 °C

2.2: 90 percent / 30 percent H₂O₂; NaOH / tetrahydrofuran / 1 h / 20 °C

With 9-borabicyclo[3.3.1]nonane dimer; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja001903v

Reference yield:

: 6972-79-8
dibenzyl glycerol

: 219744-39-5
3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaH / tetrahydrofuran

2: 1.) BH₃, 2.) H₂O₂, OH^- / 1.) THF

With borane; hydroxide; dihydrogen peroxide; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja983229b