3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

Base Information

Chemical Name:3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene
CAS No.:219744-40-8
Molecular Formula:C₈₀H₉₆O₁₄
Molecular Weight:1281.63
Hs Code.:

3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

Synonyms:3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

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Chemical Property of 3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

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Technology Process of 3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

There total 6 articles about 3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1871-57-4
2-chloromethyl-3-chloroprop-1-ene

: 219744-39-5
3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propanol

: 219744-40-8
3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja983229b

Reference yield:

: 219744-38-4
3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propene

: 219744-40-8
3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

Guidance literature:: Multi-step reaction with 2 steps

1.1: BF₃*THF / tetrahydrofuran / 5 h / 0 °C

1.2: 66 percent / sodium hydroxide; aq. hydrogen peroxide / tetrahydrofuran / 0.5 h / 20 °C

2.1: 66 percent / potassium hydroxide; 18-crown-6 / tetrahydrofuran / 2 h / 20 °C

With potassium hydroxide; boron trifluoride-tetrahydrofuran complex; 18-crown-6 ether; In tetrahydrofuran;
DOI:10.1016/j.bmc.2007.02.037

Reference yield:

: 6972-79-8
dibenzyl glycerol

: 219744-40-8
3-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxy]-2-[3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(2-benzyloxy-1-(benzyloxymethyl)ethoxymethyl)propoxymethyl]propene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95 percent / NaH / tetrahydrofuran / 20 - 65 °C

2.1: 9-BBN / tetrahydrofuran / 2 h / 0 °C

2.2: 90 percent / 30 percent H₂O₂; NaOH / tetrahydrofuran / 1 h / 20 °C

3.1: 95 percent / NaH / tetrahydrofuran / 20 - 65 °C

With 9-borabicyclo[3.3.1]nonane dimer; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja001903v