2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride

Base Information

Chemical Name:2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride
CAS No.:265130-17-4
Molecular Formula:C₇H₄Cl₃NO
Molecular Weight:224.474
Hs Code.:2928009090
DSSTox Substance ID:DTXSID40371988
Mol file:265130-17-4.mol

Synonyms:2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride;265130-17-4;DTXSID40371988;FT-0609569

Suppliers and Price of 2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
1,2',3'-TRICHLOROBENZALDOXIME 95
25g
$ 3025.00

American Custom Chemicals Corporation
1,2',3'-TRICHLOROBENZALDOXIME 95.00%
5MG
$ 501.47

Total 1 raw suppliers

Chemical Property of 2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride

Chemical Property:

Vapor Pressure:1.06E-05mmHg at 25°C
Refractive Index:1.597
Boiling Point:356.5°C at 760 mmHg
PKA:9.91±0.70(Predicted)
Flash Point:169.4°C
PSA：32.59000
Density:1.53g/cm³
LogP:3.36800
XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:222.935847
Heavy Atom Count:12
Complexity:186

Purity/Quality:: 1,2',3'-TRICHLOROBENZALDOXIME 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)Cl)C(=NO)Cl

Technology Process of 2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride

There total 2 articles about 2,3-dichloro-N-hydroxybenzenecarboximidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 4414-54-4
2,3-dichlorobenzaldehyde oxime

: 265130-17-4
2,3-dichlorobenzohydroximoyl chloride

Guidance literature:: With N-chloro-succinimide; In N,N-dimethyl-formamide; at 35 ℃; Cooling with ice;
DOI:10.1016/j.bmc.2013.07.049

Reference yield:

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 265130-17-4
2,3-dichlorobenzohydroximoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; pyridine / methanol / 2.5 h / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 35 °C / Cooling with ice

With pyridine; N-chloro-succinimide; hydroxylamine hydrochloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.07.049

Reference yield: 90.0%

: 19879-84-6
tetraacetyl thioglucose

: 265130-17-4
2,3-dichlorobenzohydroximoyl chloride

: 1454839-26-9
S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,3-dichlorophenylthiohydroxamate

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; at 20 ℃; for 2h; stereospecific reaction; Inert atmosphere;
DOI:10.1016/j.bmc.2013.07.049