(diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate

Base Information

• Chemical Name: (diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate
• CAS No.: 664980-67-0
• Molecular Formula: Ag*BF₄*C₁₈H₁₆NOP
• Molecular Weight: 487.978
• Mol file: 664980-67-0.mol

Synonyms:(diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate

Chemical Property of (diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate

There total 1 articles about (diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

silver tetrafluoroborate (14104-20-2) + diphenylphosphino-3-pyridylcarbinol (664980-65-8) → (diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate (664980-67-0)

Guidance literature:

In dichloromethane; Ar; adding 1 equiv. of Ag salt in CH2Cl2 to diphenylphosphino-3-pyridylcarbinol dissolved in CH2Cl2 under ambient temp., stiring for 5 min; solvent removal under vac., drying; elem. anal.;

DOI:10.1021/ic035168a

Reference yield:

(diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate (664980-67-0) → silver (7440-22-4)

Guidance literature:

In not given; in organic solvents;

DOI:10.1021/ic035168a

Reference yield:

dichloromethane (75-09-2) + (diphenylphosphino-3-pyridylcarbinol) tetrafluoroborate (664980-67-0) → (diphenylphosphino-3-pyridylcarbinol)AgBF4*1.5CH2Cl2

Guidance literature:

With diethyl ether; In dichloromethane; Ar; vap. diffusion of ether into dichloromethane soln. of the complex;

DOI:10.1021/ic035168a

upstream raw materials:

silver tetrafluoroborate

diphenylphosphino-3-pyridylcarbinol

Downstream raw materials:

silver