N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

Base Information

Chemical Name:N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine
CAS No.:178110-31-1
Molecular Formula:C₂₈H₂₄Cl₂N₂O₂S
Molecular Weight:523.483
Hs Code.:

Synonyms:N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

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Chemical Property of N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

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Technology Process of N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

There total 3 articles about N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 937-32-6
4-nitrobenzenesulfenyl chloride

: 178110-57-1
5'-(tert-butyl)-4,4''-dichloro-[1,1':3',1''-terphenyl]-4'-amine

: 178110-31-1
N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃; for 2h;
DOI:10.1021/jo960347d

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 178110-31-1
N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Pd(PPH₃)4, Na₂CO₃ / benzene; ethanol; H₂O / 24 h / Heating

2: 50 percent / Et₃N / diethyl ether / 2 h / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; triethylamine; In diethyl ether; ethanol; water; benzene;
DOI:10.1021/jo960347d

Reference yield:

: 94115-05-6
2,4-dibromo-6-(tert-butyl)aniline

: 178110-31-1
N-(5'-tert-Butyl-4,4''-dichloro-[1,1';3',1'']terphenyl-4'-yl)-S-(4-nitro-phenyl)-thiohydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Pd(PPH₃)4, Na₂CO₃ / benzene; ethanol; H₂O / 24 h / Heating

2: 50 percent / Et₃N / diethyl ether / 2 h / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; triethylamine; In diethyl ether; ethanol; water; benzene;
DOI:10.1021/jo960347d