1-phenyl-1,2,3-propanetriol triacetate

Base Information

Chemical Name:1-phenyl-1,2,3-propanetriol triacetate
CAS No.:101103-59-7
Molecular Formula:C₁₅H₁₈O₆
Molecular Weight:294.304
Hs Code.:

Synonyms:1-phenyl-1,2,3-propanetriol triacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-1,2,3-propanetriol triacetate

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Technology Process of 1-phenyl-1,2,3-propanetriol triacetate

There total 14 articles about 1-phenyl-1,2,3-propanetriol triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 300-57-2,57807-91-7
allylbenzene

: 108-24-7
acetic anhydride

: 86551-93-1,51759-70-7
acetic acid 2-acetoxy-3-phenyl-propyl ester

: 65870-47-5,65870-50-0,86594-56-1,101103-59-7,116127-77-6
syn-acetic acid 2,3-diacetoxy-1-phenylpropyl ester

Guidance literature:: With peracetic acid; palladium diacetate; acetic acid; at 60 ℃; for 0.0833333h; Green chemistry;
DOI:10.1021/ol3026445

Reference yield: 72.0%

: 108-24-7
acetic anhydride

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 65870-47-5,65870-50-0,86594-56-1,101103-59-7,116127-77-6
syn-acetic acid 2,3-diacetoxy-1-phenylpropyl ester

Guidance literature:: (2E)-3-phenyl-2-propen-1-ol; With trifluorormethanesulfonic acid; 4-tolyl iodide; dihydrogen peroxide; acetic anhydride; In dichloromethane; acetic acid; at 20 ℃; for 24h;

acetic anhydride; With pyridine; at 20 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol301311e

Reference yield: 71.0%

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 104-54-1
3-Phenylpropenol

: 108-24-7
acetic anhydride

: 64-19-7,77671-22-8
acetic acid

: 65870-47-5,65870-50-0,86594-56-1,101103-59-7,116127-77-6
syn-acetic acid 2,3-diacetoxy-1-phenylpropyl ester

Guidance literature:: [bis(acetoxy)iodo]benzene; 3-Phenylpropenol; acetic acid; With boron trifluoride diethyl etherate; In water; at 20 ℃; for 24h;

acetic anhydride; With pyridine; at 20 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/jo201752y