N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide

Base Information

• Chemical Name: N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide
• CAS No.: 28005-57-4
• Molecular Formula: C₁₇H₁₇NO₃S
• Molecular Weight: 315.393
• Mol file: 28005-57-4.mol

Synonyms:N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide

Chemical Property of N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide

There total 4 articles about N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

ethanol (64-17-5) + 2-(4-methoxyphenyl)-4H-3,1-benzothiazin-4-one (85094-63-9) → N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide (28005-57-4)

Guidance literature:

With sodium; for 0.5h; Ambient temperature;

Reference yield:

methyl 2-isothiocyanatobenzoate (16024-82-1) → N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide (28005-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: anhydrous aluminum chloride / 1.) room temp., 1 h; 2.) conc. HCl, water

2: 91 percent / sodium / 0.5 h / Ambient temperature

With aluminium trichloride; sodium;

Reference yield:

methoxybenzene (100-66-3) → N-(2-ethoxycarbonylphenyl)-4-methoxythiobenzamide (28005-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: anhydrous aluminum chloride / 1.) room temp., 1 h; 2.) conc. HCl, water

2: 91 percent / sodium / 0.5 h / Ambient temperature

With aluminium trichloride; sodium;

upstream raw materials:

ethanol

2-(4-methoxyphenyl)-4H-3,1-benzothiazin-4-one

methyl 2-isothiocyanatobenzoate

methoxybenzene

Downstream raw materials:

2-(4-methoxyphenyl)-3H-quinazolin-4-one

3-hydroxy-2-(4-methoxyphenyl)-4(3H)-quinazolinone

2-(4-methoxyphenyl)-4H-3,1-benzothiazin-4-one

3-amino-2-(4-methoxyphenyl)-4(3H)-quinazolinone