ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate

Base Information

• Chemical Name: ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate
• CAS No.: 290332-75-1
• Molecular Formula: C₂₀H₃₀N₂O₇S
• Molecular Weight: 442.533

Synonyms:ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate

Chemical Property of ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate

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Technology Process of ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate

There total 2 articles about ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

ethyl 2-(chlorosulfonyl)acetate (55896-93-0) + tert-butyl 4-(4-aminophenoxy)piperidine-1-carboxylate (138227-63-1) → ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate (290332-75-1)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 13h;

DOI:10.1248/cpb.56.758

Reference yield: 75.0%

ethyl 2-(chlorosulfonyl)acetate (55896-93-0) + ethyl acetate (141-78-6) + tert-butyl 4-(4-aminophenoxy)piperidine-1-carboxylate (138227-63-1) → ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate (290332-75-1)

Guidance literature:

With pyridine; In methanol; hexane; dichloromethane;

Reference yield: 93.0%

3-(3-cyano-4-fluorophenyl)-2-(E)-propen-1-ol (337519-96-7) + ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}sulfamoyl)acetate (290332-75-1) + ethyl acetate (141-78-6) + diethylazodicarboxylate (1972-28-7,218603-74-8) → Ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)phenyl]-N-[3-(3-cyano-4-fluorophenyl)-2-(E)-propenyl]sulfamoylacetate (337519-97-8)

Guidance literature:

With triphenylphosphine; In dichloromethane;

upstream raw materials:

ethyl 2-(chlorosulfonyl)acetate

tert-butyl 4-(4-aminophenoxy)piperidine-1-carboxylate

ethyl acetate

Downstream raw materials:

ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)phenyl]-N-[3-(3-cyanophenyl)-2-fluoro-2-(Z)-propenyl]sulfamoylacetate

ethyl (N-{4-[1-(t-butoxycarbonyl)piperidin-4-yloxy]phenyl}-N-[(E)-3-(3-cyanophenyl)-2-propenyl]sulfamoyl)acetate

Ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)phenyl]-N-[3-(3-cyano-5-methylphenyl)-2-(E)-propenyl]sulfamoylacetate

Ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)phenyl]-N-[3-(3-cyano-4-fluorophenyl)-2-(E)-propenyl]sulfamoylacetate

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