C₂₉H₄₂N₂O₄

Base Information

Chemical Name:C₂₉H₄₂N₂O₄
CAS No.:1179810-90-2
Molecular Formula:C₂₉H₄₂N₂O₄
Molecular Weight:482.663
Hs Code.:

C<sub>29</sub>H<sub>42</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₉H₄₂N₂O₄

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Chemical Property of C₂₉H₄₂N₂O₄

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Technology Process of C₂₉H₄₂N₂O₄

There total 8 articles about C₂₉H₄₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1180022-76-7
1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

: 1179810-90-2
C₂₉H₄₂N₂O₄

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In ethanol; at 0 ℃; for 0.166667h; Inert atmosphere;

Reference yield:

: 207681-67-2
N-methoxy-N-methyl-3-bromobenzamide

: 1179810-90-2
C₂₉H₄₂N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / n-heptane; diethyl ether; tetrahydrofuran / -78 - -50 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: ethanol; sodium tetrahydroborate / 3 h / 20 °C

3.1: formic acid / 24 h / Reflux

3.2: 3 h / 20 °C

3.3: pH 1

4.1: thionyl chloride / 2 h / 60 °C / Inert atmosphere

4.2: 1 h / 20 °C

5.1: potassium carbonate; silver(l) oxide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube

5.2: 2 h

6.1: tetrahydrofuran / 48 h / Reflux; Inert atmosphere

7.1: acetic acid; sodium tris(acetoxy)borohydride / ethanol / 0.17 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; formic acid; thionyl chloride; ethanol; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; silver(l) oxide; lithium diisopropyl amide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; diethyl ether; ethanol; n-heptane;

Reference yield:

: 1179811-05-2
4-(3-bromobenzoyl)nicotinic acid

: 1179810-90-2
C₂₉H₄₂N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / 2 h / 60 °C / Inert atmosphere

1.2: 1 h / 20 °C

2.1: potassium carbonate; silver(l) oxide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube

2.2: 2 h

3.1: tetrahydrofuran / 48 h / Reflux; Inert atmosphere

4.1: acetic acid; sodium tris(acetoxy)borohydride / ethanol / 0.17 h / 0 °C / Inert atmosphere

With thionyl chloride; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; silver(l) oxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; ethanol;