N2,N2,N4,N4-TETRAMETHYL-6-CHLORO-1,3,5-TRIAZINE-2,4-DIAMINE

Base Information

• Chemical Name: N2,N2,N4,N4-TETRAMETHYL-6-CHLORO-1,3,5-TRIAZINE-2,4-DIAMINE
• CAS No.: 3140-74-7
• Molecular Formula: C7H12 Cl N5
• Molecular Weight: 201.659
• Hs Code.: 2933699090
• Mol file: 3140-74-7.mol

Synonyms:1,3,5-Triazine-2,4-diamine,6-chloro-N,N,N',N'-tetramethyl- (9CI); s-Triazine, 2-chloro-4,6-bis(dimethylamino)-(7CI,8CI); 2,4-Bis(dimethylamino)-6-chloro-1,3,5-triazine;2,4-Bis(dimethylamino)-6-chloro-s-triazine;2-Chloro-4,6-bis(dimethylamino)-1,3,5-triazine;2-Chloro-4,6-bis(dimethylamino)-s-triazine;6-Chloro-2,4-bis(dimethylamino)-1,3,5-triazine;N,N,N',N'-Tetramethyl-6-chloro-[1,3,5]triazine-2,4-diamine

Chemical Property of N2,N2,N4,N4-TETRAMETHYL-6-CHLORO-1,3,5-TRIAZINE-2,4-DIAMINE

Chemical Property:

• PSA: 45.15000
• LogP: 0.65700

Purity/Quality:

98% ^*data from raw suppliers

6-?Chloro-?2-?N,?2-?N,?4-?N,?4-?N-?tetramethyl-?1,?3,?5-?triazine-?2,?4-?diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 6-?Chloro-?2-?N,?2-?N,?4-?N,?4-?N-?tetramethyl-?1,?3,?5-?triazine-?2,?4-?diamine is a reagent used in the preparation of temperature and pH responsive starches.

Technology Process of N2,N2,N4,N4-TETRAMETHYL-6-CHLORO-1,3,5-TRIAZINE-2,4-DIAMINE

There total 7 articles about N2,N2,N4,N4-TETRAMETHYL-6-CHLORO-1,3,5-TRIAZINE-2,4-DIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + dimethyl amine (124-40-3) → 2-chloro-4,6-bis(dimethylamino)-1,3,5-triazine (3140-74-7)

Guidance literature:

In water; acetone; a) 0 deg C, 2 h, b) RT, 18 h;

DOI:10.1248/cpb.45.291

Reference yield: 90.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + N,N-dimethylammonium chloride (506-59-2) → 2-chloro-4,6-bis(dimethylamino)-1,3,5-triazine (3140-74-7)

Guidance literature:

With sodium hydroxide; In acetone; at 20 - 50 ℃; for 1.5h;

DOI:10.1021/jm050177+

Reference yield: 69.0%

N-cyano-N’,N’-dimethylguanidine (1609-06-9) + dichloromethylenedimethyliminium chloride (33842-02-3,529510-96-1) → 2-chloro-4,6-bis(dimethylamino)-1,3,5-triazine (3140-74-7)

Guidance literature:

In acetonitrile; for 0.5h; Heating;

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

dimethyl amine

N-cyano-N’,N’-dimethylguanidine

dichloromethylenedimethyliminium chloride

Downstream raw materials:

N-<4,6-bis(dimethylamino)-1,3,5-triazin-2-yl>trimethylammonium chloride

Refernces

• 1、 Zeng, Yingying,Pratumyot, Yaowalak,Piao, Xijun,Bong, Dennis. "Discrete assembly of synthetic peptide-DNA triplex structures from polyvalent melamine-thymine bifacial recognition". . p. 832 - 835. Retrieved 2012.
• 2、 -. "Application of heterocyclic thiol compound in preparation of antitumor drugs". Paragraph 0024-0025; 0031-0032. . Retrieved 2021/08/25.
• 3、 List, Manuela,Puchinger, Helmut,Gabriel, Herbert,Monkowius, Uwe,Schwarzinger, Clemens. "N-Methylmelamines: Synthesis, Characterization, and Physical Properties". . p. 4066 - 4075. Retrieved 2016/06/09.