(2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

Base Information

Chemical Name:(2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane
CAS No.:146499-48-1
Molecular Formula:C₂₉H₃₉NO₆S₂Si
Molecular Weight:589.849
Hs Code.:

Synonyms:(2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

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Chemical Property of (2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

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Technology Process of (2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

There total 7 articles about (2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 146499-48-1
(2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 19 h / Ambient temperature

2: 1.33 g / 5percent Pd-C, HCO₂NH₄ / methanol / 1 h / Ambient temperature

3: Et₃N, DMAP / CH₂Cl₂ / 3 h / Ambient temperature

With 1H-imidazole; dmap; palladium on activated charcoal; ammonium formate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80749-3

Reference yield:

: 156350-20-8
Toluene-4-sulfonic acid (2R,3R)-3-azido-2-hydroxy-3-phenyl-propyl ester

: 146499-48-1
(2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 19 h / Ambient temperature

2: 1.33 g / 5percent Pd-C, HCO₂NH₄ / methanol / 1 h / Ambient temperature

3: Et₃N, DMAP / CH₂Cl₂ / 3 h / Ambient temperature

With 1H-imidazole; dmap; palladium on activated charcoal; ammonium formate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80749-3

Reference yield:

: 146499-47-0
(2R,3R)-3-azido-2-tert-butyldimethylsiloxy-3-phenyl-1-p-toluenesulfonyloxypropane

: 146499-48-1
(2R,3R)-2-tert-butyldimethylsiloxy-3-phenyl-3-p-toluenesulfonylamino-1-p-toluenesulfonylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.33 g / 5percent Pd-C, HCO₂NH₄ / methanol / 1 h / Ambient temperature

2: Et₃N, DMAP / CH₂Cl₂ / 3 h / Ambient temperature

With dmap; palladium on activated charcoal; ammonium formate; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)80749-3