(E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

Base Information

Chemical Name:(E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol
CAS No.:1268468-00-3
Molecular Formula:C₁₇H₁₈O₃
Molecular Weight:270.328
Hs Code.:

Synonyms:(E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

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Chemical Property of (E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

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Technology Process of (E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

There total 5 articles about (E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 50415-62-8,693775-75-6
methyl (E)-4-methoxy-α-(4'-methoxyphenylmethylene)benzeneacetate

: 1268468-00-3
(E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

Guidance literature:: methyl (E)-4-methoxy-α-(4'-methoxyphenylmethylene)benzeneacetate; With aluminum (III) chloride; lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 2.16667h; Inert atmosphere;

With water; In diethyl ether; for 0.5h; Cooling; Inert atmosphere;
DOI:10.1002/anie.201006292

Reference yield: 78.0%

: 64-18-6
formic acid

: 2132-62-9
4,4'-dimethoxydiphenylacetylene

: 1268468-00-3
(E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

Guidance literature:: 4,4'-dimethoxydiphenylacetylene; With cesium acetate; copper diacetate; [(4S)-4-[5-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphanyl-1,3-benzodioxol-4-yl]-4,5,6,7-tetrahydro-1,3-benzodioxol-5-yl]-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphane; In cyclohexane; for 0.5h; Glovebox; Schlenk technique; Inert atmosphere;

formic acid; With Triethoxysilane; In cyclohexane; at 55 ℃; for 24h; Inert atmosphere; Sealed tube; Schlenk technique;

With ammonium fluoride; In methanol; at 20 ℃; for 0.25h; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.1c01473

Reference yield: 51.0%

: 124-38-9,18923-20-1
carbon dioxide

: 2132-62-9
4,4'-dimethoxydiphenylacetylene

: 1268468-00-3
(E)-2,3-bis(4-methoxyphenyl)prop-2-en-1-ol

Guidance literature:: With Triethoxysilane; ((4,4'-bi-1,3-benzodioxole)-5,5'-diyl)bis(bis(3,5-di-tert-butylphenyl)phosphine); cesium acetate; copper diacetate; In cyclohexane; at 60 ℃; for 25h; under 760.051 Torr; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202012768