1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol

Base Information

Chemical Name:1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol
CAS No.:373606-49-6
Molecular Formula:C₂₆H₃₆O₄Si
Molecular Weight:440.655
Hs Code.:

Synonyms:1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol

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Chemical Property of 1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol

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Technology Process of 1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol

There total 1 articles about 1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 81928-98-5
4,6-di-O-benzyl-D-galactal

: 18162-48-6
tert-butyldimethylsilyl chloride

: 373606-49-6
1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 1.5h;
DOI:10.1021/jo015987h

Reference yield: 73.0%

: 3282-30-2
pivaloyl chloride

: 107-66-4
dibutyl phosphate

: 373606-49-6
1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol

: 373606-20-3
dibutyl 3-O-tert-butyldimethylsilyl-4,6-di-O-benzyl-2-O-pivaloyl-β-D-galactopyranosyl phosphate

Guidance literature:: 1,5-anhydro-3-O-tert-butyldimethylsilyl-2-deoxy-4,6-di-O-benzyl-D-lyxo-hex-1-enitol; With 3,3-dimethyldioxirane; In dichloromethane; acetone; at 0 ℃; for 0.333333h;

dibutyl phosphate; In dichloromethane; at -78 ℃; for 0.25h;

pivaloyl chloride; With dmap; In dichloromethane; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1021/jo015987h