(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

Base Information

Chemical Name:(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate
CAS No.:1522124-83-9
Molecular Formula:C₁₉H₂₃N₂O₇P
Molecular Weight:422.375
Hs Code.:

Synonyms:(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

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Chemical Property of (S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

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Technology Process of (S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

There total 4 articles about (S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1522124-82-8
(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dibenzyl phosphate

: 1522124-83-9
(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

Guidance literature:: With hydrogen; palladium; In water; tert-butyl alcohol; at 20 ℃; for 12h; Solvent; Reagent/catalyst; Temperature; Inert atmosphere;
DOI:10.1021/ja411737c

Reference yield:

: 1522124-79-3
(S)-N-(3-hydroxy-1-((4-methoxyphenethyl)amino)-1-oxopropan-2-yl)benzamide

: 1522124-83-9
(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / dichloromethane; acetonitrile / 5 h / 20 °C

1.2: 3 h / -40 - 20 °C

2.1: palladium; hydrogen / water; tert-butyl alcohol / 12 h / 20 °C / Inert atmosphere

With 1H-tetrazole; hydrogen; palladium; In dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja411737c

Reference yield:

: 98-88-4
benzoyl chloride

: 1522124-83-9
(S)-2-benzamido-3-((4-methoxyphenethyl)amino)-3-oxopropyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / water / 16 h / 20 °C / pH 3 - 4

2.1: tetrahydrofuran / 0.03 h / -78 °C / Inert atmosphere

2.2: 0.03 h / Inert atmosphere

2.3: 3 h / -78 - 20 °C / Inert atmosphere

3.1: 1H-tetrazole / dichloromethane; acetonitrile / 5 h / 20 °C

3.2: 3 h / -40 - 20 °C

4.1: palladium; hydrogen / water; tert-butyl alcohol / 12 h / 20 °C / Inert atmosphere

With 1H-tetrazole; hydrogen; potassium carbonate; palladium; In tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja411737c