Technology Process of 2-methoxy-3,6-dimethyl-5-nitrohydroquinone dibenzyl ether
There total 6 articles about 2-methoxy-3,6-dimethyl-5-nitrohydroquinone dibenzyl ether which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) nitrate;
In
acetic anhydride;
for 0.5h;
DOI:10.1248/cpb.33.2122
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 66 percent / acetic acid / 2 h / Heating
2: 86 percent / hydrazine hydrate, KOH / 1.) reflux, 15 min; 2.) 120 deg C, 30 min; 3.) 140 deg C, 30 min
3: 77 percent / ceric ammonium nitrate / H2O; acetonitrile / 0.75 h / Ambient temperature
4: sodium dithionite / H2O; diethyl ether / 2 h
5: 57 percent / anhydrous K2CO3 / dimethylformamide / 18 h / Ambient temperature
6: 44 percent / cupric nitrate trihydrate / acetic anhydride / 0.5 h
With
potassium hydroxide; sodium dithionite; ammonium cerium(IV) nitrate; potassium carbonate; copper(II) nitrate; hydrazine hydrate;
In
diethyl ether; water; acetic anhydride; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.33.2122
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / ceric ammonium nitrate / H2O; acetonitrile / 0.75 h / Ambient temperature
2: sodium dithionite / H2O; diethyl ether / 2 h
3: 57 percent / anhydrous K2CO3 / dimethylformamide / 18 h / Ambient temperature
4: 44 percent / cupric nitrate trihydrate / acetic anhydride / 0.5 h
With
sodium dithionite; ammonium cerium(IV) nitrate; potassium carbonate; copper(II) nitrate;
In
diethyl ether; water; acetic anhydride; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.33.2122
