2-methoxy-3,6-dimethylhydroquinone dibenzyl ether

Base Information

Chemical Name:2-methoxy-3,6-dimethylhydroquinone dibenzyl ether
CAS No.:100827-51-8
Molecular Formula:C₂₃H₂₄O₃
Molecular Weight:348.442
Hs Code.:

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Chemical Property of 2-methoxy-3,6-dimethylhydroquinone dibenzyl ether

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Technology Process of 2-methoxy-3,6-dimethylhydroquinone dibenzyl ether

There total 5 articles about 2-methoxy-3,6-dimethylhydroquinone dibenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 99892-95-2
2-methoxy-3,6-dimethylhydroquinone

: 100-39-0
benzyl bromide

: 100827-51-8
2-methoxy-3,6-dimethylhydroquinone dibenzyl ether

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1248/cpb.33.2122

Reference yield:

: 19676-67-6
2,4-dimethoxy-3-methylphenol

: 100827-51-8
2-methoxy-3,6-dimethylhydroquinone dibenzyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / acetic acid / 2 h / Heating

2: 86 percent / hydrazine hydrate, KOH / 1.) reflux, 15 min; 2.) 120 deg C, 30 min; 3.) 140 deg C, 30 min

3: 77 percent / ceric ammonium nitrate / H₂O; acetonitrile / 0.75 h / Ambient temperature

4: sodium dithionite / H₂O; diethyl ether / 2 h

5: 57 percent / anhydrous K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

With potassium hydroxide; sodium dithionite; ammonium cerium(IV) nitrate; potassium carbonate; hydrazine hydrate; In diethyl ether; water; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.33.2122

Reference yield:

: 53887-75-5
2,4-dimethoxy-3,6-dimethylphenol

: 100827-51-8
2-methoxy-3,6-dimethylhydroquinone dibenzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / ceric ammonium nitrate / H₂O; acetonitrile / 0.75 h / Ambient temperature

2: sodium dithionite / H₂O; diethyl ether / 2 h

3: 57 percent / anhydrous K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

With sodium dithionite; ammonium cerium(IV) nitrate; potassium carbonate; In diethyl ether; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.33.2122