(1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

Base Information

Chemical Name:(1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride
CAS No.:1235545-48-8
Molecular Formula:C₂₁H₂₂F₂N₂O₂*ClH
Molecular Weight:408.876
Hs Code.:

Synonyms:(1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

Chemical Property:

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Technology Process of (1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

There total 3 articles about (1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1235545-49-9
tert-butyl 9H-fluoren-9-ylmethyl [(1S,2R)-3,3-difluorocyclohexane-1,2-diyl]biscarbamate

: 1235545-48-8
(1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 50 ℃;

Reference yield:

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1235545-48-8
(1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetonitrile; water / 1.5 h

2: hydrogenchloride / 1,4-dioxane / 2 h / 50 °C

With hydrogenchloride; sodium hydrogencarbonate; In 1,4-dioxane; water; acetonitrile;

Reference yield:

: 1109284-47-0
tert-butyl [(1R,6S)-6-amino-2,2-difluorocyclohexyl]carbamate

: 1235545-48-8
(1R,6S)-6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-2,2-difluorocyclohexanaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetonitrile; water / 1.5 h

2: hydrogenchloride / 1,4-dioxane / 2 h / 50 °C

With hydrogenchloride; sodium hydrogencarbonate; In 1,4-dioxane; water; acetonitrile;