Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

Base Information

Chemical Name:Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester
CAS No.:109720-12-9
Molecular Formula:C₉H₁₀N₂O₂S₂
Molecular Weight:242.323
Hs Code.:

Synonyms:Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

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Chemical Property of Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

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Technology Process of Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

There total 3 articles about Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 75-15-0,12122-00-8
carbon disulfide

: 124-40-3
dimethyl amine

: 99-09-2
3-nitro-aniline

: 109720-12-9
Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

Guidance literature:: 3-nitro-aniline; With sodium nitrite; In water; at 20 ℃; for 0.166667h; Milling; Green chemistry;

carbon disulfide; dimethyl amine; In water; at 20 ℃; for 0.25h; Green chemistry;
DOI:10.1080/10426507.2015.1024311

Reference yield: 63.0%

: 6293-62-5
bis-(3-nitro-phenyl)-iodonium ; chloride

: 128-04-1
sodium dimethyldithiocarbamate

: 109720-12-9
Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

Guidance literature:: In acetonitrile; at 70 ℃; for 3h;
DOI:10.1021/jo00227a032

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 586-36-7
3-nitrophenyldiazonium tetrafluoroborate

: 124-40-3
dimethyl amine

: 109720-12-9
Dimethyl-dithiocarbamic acid 3-nitro-phenyl ester

Guidance literature:: carbon disulfide; dimethyl amine; In water; at 0 - 5 ℃; for 0.0833333h; Inert atmosphere;

3-nitrophenyldiazonium tetrafluoroborate; In water; at 0 - 25 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c9ob01976f