Rh(ttp)CH₂COPh

Base Information

• Chemical Name: Rh(ttp)CH₂COPh
• CAS No.: 1247874-33-4
• Molecular Formula: C₅₆H₄₃N₄ORh
• Molecular Weight: 890.889

Synonyms:Rh(ttp)CH₂COPh

Chemical Property of Rh(ttp)CH₂COPh

Chemical Property:

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Technology Process of Rh(ttp)CH₂COPh

There total 5 articles about Rh(ttp)CH₂COPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(5,10,15,20-tetrakis-4-tolylporphyrinato)(methyl)rhodium(III) (103533-61-5) + acetophenone (98-86-2) → Rh(ttp)CH2COPh (1247874-33-4)

Guidance literature:

In neat (no solvent); (N2); heating of Rh(5,10,15,20-tetratolylporphyrinato)Me and acetophenone at 200°C under N2 for 3 ds in the dark; drying under vac., silica gel column chromy. with hexane/CH2Cl2 as eluent;

DOI:10.1021/om200788p

Reference yield:

(5,10,15,20-tetrakis-4-tolylporphyrinato)(methyl)rhodium(III) (103533-61-5) + acetophenone (98-86-2) → methane (34557-54-5,27936-85-2) + (5,10,15,20-tetrakis-4-tolylporphyrinato)rhodium(III) hydride (103562-44-3) + Rh(ttp)CH2COPh (1247874-33-4)

Guidance literature:

In benzene-d6; at 200 ℃; for 0.5h; Inert atmosphere; Darkness;

DOI:10.1021/om200788p

Reference yield:

(5,10,15,20-tetrakis-4-tolylporphyrinato)(methyl)rhodium(III) (103533-61-5) + acetophenone (98-86-2) → (5,10,15,20-tetrakis-4-tolylporphyrinato)rhodium(III) hydride (103562-44-3) + Rh(ttp)CH2COPh (1247874-33-4)

Guidance literature:

In benzene-d6; byproducts: CH4; soln. of Rh complex and ketone in C6D6 was heated at 200°C for 30min;

DOI:10.1021/om1007852

upstream raw materials:

(5,10,15,20-tetrakis-4-tolylporphyrinato)(methyl)rhodium(III)

acetophenone

Downstream raw materials:

(5,10,15,20-tetrakis-4-tolylporphyrinato)rhodium(III) hydride

acetophenone

(5,10,15,20-tetratolylporphyrinato)(benzoyl)rhodium(III)

1,3,5-triphenylbenzene

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