C₁₆H₁₇BrO₆

Base Information

Chemical Name:C₁₆H₁₇BrO₆
CAS No.:1373610-44-6
Molecular Formula:C₁₆H₁₇BrO₆
Molecular Weight:385.211
Hs Code.:

C<sub>16</sub>H<sub>17</sub>BrO<sub>6</sub>

Synonyms:C₁₆H₁₇BrO₆

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Chemical Property of C₁₆H₁₇BrO₆

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Technology Process of C₁₆H₁₇BrO₆

There total 3 articles about C₁₆H₁₇BrO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1373610-47-9
(2R,3R,4R)-2-ethyl 4-methyl 5-oxo-3-phenyltetrahydrofuran-2,4-dicarboxylate

: 74-95-3
1,1-dibromomethane

: 1373610-44-6
C₁₆H₁₇BrO₆

Guidance literature:: With 18-crown-6 ether; potassium carbonate; at 20 ℃; for 36h;
DOI:10.1021/ja3027136

Reference yield:

: 6626-84-2
dimethyl 2-benzylidenepropanedioate

: 1373610-44-6
C₁₆H₁₇BrO₆

Guidance literature:: Multi-step reaction with 3 steps

1: 2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; triethylamine / toluene / 16 h / 20 °C / Inert atmosphere

2: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; formic acid; C40H32N2O2S; triethylamine / N,N-dimethyl-formamide / 16.5 h / 20 - 70 °C / Inert atmosphere; Resolution of racemate

3: 18-crown-6 ether; potassium carbonate / 36 h / 20 °C

With 2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; formic acid; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 18-crown-6 ether; C₄₀H₃₂N₂O₂S; potassium carbonate; triethylamine; In N,N-dimethyl-formamide; toluene; 1: Stetter reaction;
DOI:10.1021/ja3027136

Reference yield:

: 1373610-31-1
1-ethyl 3,3-dimethyl 1-oxo-2-phenylpropane-1,3,3-tricarboxylate

: 1373610-44-6
C₁₆H₁₇BrO₆

Guidance literature:: Multi-step reaction with 2 steps

1: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; formic acid; C40H32N2O2S; triethylamine / N,N-dimethyl-formamide / 16.5 h / 20 - 70 °C / Inert atmosphere; Resolution of racemate

2: 18-crown-6 ether; potassium carbonate / 36 h / 20 °C

With formic acid; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 18-crown-6 ether; C₄₀H₃₂N₂O₂S; potassium carbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja3027136