1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether

Base Information

Chemical Name:1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether
CAS No.:1025691-16-0
Molecular Formula:C₁₅H₃₂OSi₂
Molecular Weight:284.589
Hs Code.:

Synonyms:1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether

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Chemical Property of 1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether

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Technology Process of 1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether

There total 1 articles about 1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 930-68-7
cyclohexenone

: 18162-48-6
tert-butyldimethylsilyl chloride

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1025691-16-0
1-tert-butyldimethylsilyl 3-(trimethylsilyl)cyclohexenyl ether

Guidance literature:: 1,1,1,3,3,3-hexamethyl-disilazane; With methyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; at -78 - 0 ℃; Inert atmosphere;

cyclohexenone; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; for 0.0833333h; Inert atmosphere;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol800007v