1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Base Information

Chemical Name:1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine
CAS No.:960595-40-8
Molecular Formula:C₁₆H₂₅NOSi
Molecular Weight:275.466
Hs Code.:

Synonyms:1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Suppliers and Price of 1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

There total 1 articles about 1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 31007-06-4
2-(4-methoxyphenyl)propionitrile

: 18162-48-6
tert-butyldimethylsilyl chloride

: 960595-40-8
1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Guidance literature:: 2-(4-methoxyphenyl)propionitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201403342

Reference yield: 97.0%

: 960595-40-8
1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

: 1373942-84-7
tert-butyl (1-benzyl-2-oxoindolin-3-ylidene)carbamate

: tert-butyl (1-benzyl-3-(1-cyano-1-(4-methoxyphenyl)ethyl)-2-oxoindolin-3-yl)carbamate

Guidance literature:: With C₃₁H₄₀N₄O₄; zinc trifluoromethanesulfonate; In tetrahydrofuran; at -45 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201408730

Reference yield: 90.0%

: 960595-40-8
1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine

: 100-52-7
benzaldehyde

: 960595-22-6
(2R,3S)-3-hydroxy-2-(4-methoxyphenyl)-2-methyl-3-phenylpropanenitrile

: C₁₇H₁₇NO₂

Guidance literature:: 1-(1,1-dimethylethyl)-N-[2-(4-methoxyphenyl)-1-propenylidene]-1,1-dimethylsilanamine; benzaldehyde; With tetrachlorosilane; chiral bisphosphoramide catalyst; In dichloromethane; at -78 ℃; for 2h;

With potassium fluoride; sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 3h; Further stages.;
DOI:10.1021/ja077134y