(Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

Base Information

Chemical Name:(Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate
CAS No.:1438409-27-8
Molecular Formula:C₂₉H₂₆N₂O₅S
Molecular Weight:514.602
Hs Code.:

Synonyms:(Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

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Chemical Property of (Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

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Technology Process of (Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

There total 4 articles about (Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.4%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1438408-95-7
(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

: 1438409-27-8
(Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1039/c3ob40199e

Reference yield:

: (Z)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione

: 1438409-27-8
(Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine / tetrahydrofuran / 0.08 h / 20 °C

1.2: 45 °C

2.1: dichloromethane / 0.5 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob40199e

Reference yield:

: 1438408-80-0
C₃₃H₃₀N₂O₃S

: 1438409-27-8
(Z)-(9H-fluoren-9-yl)methyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0.5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/c3ob40199e