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Technology Process of Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2

Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2

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  • Chemical Name:Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2
  • CAS No.:377774-29-3
  • Molecular Formula:C33H57Cl4LiN2O2Si2Zr
  • Molecular Weight:809.976
  • Hs Code.:
Zr(N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)C(Si(CH<sub>3</sub>)3)C(H)C(Si(CH<sub>3</sub>)3)N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2))Cl<sub>4</sub>Li(O(C<sub>2</sub>H<sub>5</sub>)2)2

Synonyms:Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2

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Chemical Property of Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2
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Technology Process of Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2

There total 1 articles about Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.2%

diethyl ether
60-29-7,927820-24-4

diethyl ether

Li(N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)C(Si(CH<sub>3</sub>)3)C(H)C(Si(CH<sub>3</sub>)3)N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2))
203522-22-9

Li(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))

zirconium(IV) chloride
10026-11-6

zirconium(IV) chloride

Zr(N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)C(Si(CH<sub>3</sub>)3)C(H)C(Si(CH<sub>3</sub>)3)N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2))Cl<sub>4</sub>Li(O(C<sub>2</sub>H<sub>5</sub>)2)2
377774-29-3

Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2

Guidance literature:
In diethyl ether; under N2, standard Schlenk techniques; ZrCl4 added at -78°C to soln. of Li compd. (molar ratio 1:1) in Et2O; warmed to room temp.; stirred for 14 h; filtered; filtrate cooled; another crop of crystals obtained from motherliquor; elem. anal.;
DOI:10.1039/b103553n

Reference yield:

Zr(N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)C(Si(CH<sub>3</sub>)3)C(H)C(Si(CH<sub>3</sub>)3)N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2))Cl<sub>4</sub>Li(O(C<sub>2</sub>H<sub>5</sub>)2)2
377774-29-3

Zr(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))Cl4Li(O(C2H5)2)2

zirconium
7440-67-7

zirconium

Li(N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)C(Si(CH<sub>3</sub>)3)C(H)C(Si(CH<sub>3</sub>)3)N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2))
203522-22-9

Li(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))

Guidance literature:
With CH3Li; In not given; under N2, standard Schlenk techniques; treated with MeLi;
DOI:10.1039/b103553n
upstream raw materials:

diethyl ether

Li(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))

zirconium(IV) chloride

Downstream raw materials:

zirconium

Li(N(C6H3(CH3)2)C(Si(CH3)3)C(H)C(Si(CH3)3)N(C6H3(CH3)2))

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