10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

Base Information

Chemical Name:10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide
CAS No.:1383710-76-6
Molecular Formula:C₂₇H₃₂ClN₂*I
Molecular Weight:546.922
Hs Code.:

Synonyms:10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

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Chemical Property of 10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

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Technology Process of 10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

There total 8 articles about 10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-50-0
cyclohexylmagnesium bromide

: 1383710-76-6
10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: dilithium tetrachlorocuprate / tetrahydrofuran; diethyl ether / 0.42 h / 5 - 10 °C / Inert atmosphere

1.2: 13.5 h / 0 - 20 °C

2.1: sodium iodide / acetone / 12 h / 60 °C

3.1: sodium hydride / 1,2-dimethoxyethane / 12 h / 20 °C

4.1: toluene / 24 h / 110 °C / Sealed tube

With dilithium tetrachlorocuprate; sodium hydride; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; acetone; toluene;

Reference yield:

: 1383710-80-2
10-chloro-7-(5-cyclohexyl-pentyl)-7H-indolo[2,3-c]-quinoline

: 74-88-4
methyl iodide

: 1383710-76-6
10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

Guidance literature:: In toluene; at 110 ℃; for 24h; Sealed tube;

Reference yield:

: 580-17-6
3-aminoquinoline

: 1383710-76-6
10-Chloro-7-(5-cyclohexyl-pentyl)-5-methyl-7H-indolo[2,3-c]quinolin-5-ium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / copper diacetate / dichloromethane / 20 °C / Molecular sieve

2: trifluoroacetic acid / palladium diacetate / 6 h / 80 °C

3: sodium hydride / 1,2-dimethoxyethane / 12 h / 20 °C

4: toluene / 24 h / 110 °C / Sealed tube

With sodium hydride; triethylamine; trifluoroacetic acid; copper diacetate; palladium diacetate; In 1,2-dimethoxyethane; dichloromethane; toluene;