N-(4-iodophenyl)-4-methoxybenzenesulfonamide

Base Information

Chemical Name:N-(4-iodophenyl)-4-methoxybenzenesulfonamide
CAS No.:314054-03-0
Molecular Formula:C₁₃H₁₂INO₃S
Molecular Weight:389.214
Hs Code.:
Mol file:314054-03-0.mol

Synonyms:N-(4-iodo-phenyl)-4-methoxy-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-iodophenyl)-4-methoxybenzenesulfonamide

Chemical Property:

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Technology Process of N-(4-iodophenyl)-4-methoxybenzenesulfonamide

There total 1 articles about N-(4-iodophenyl)-4-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 540-37-4
p-aminoiodobenzene

: 314054-03-0
N-(4-iodo-phenyl)-4-methoxy-benzenesulfonamide

Guidance literature:: 4-methoxy-phenyl-sulphonyl chloride; p-aminoiodobenzene; With triethylamine; In dichloromethane;

With sodium methylate; In methanol;
DOI:10.1016/S0960-894X(01)00552-2

Reference yield:

: 79-10-7
acrylic acid

: 314054-03-0
N-(4-iodo-phenyl)-4-methoxy-benzenesulfonamide

: 501682-94-6
(E)-3-[4-(4-Methoxy-benzenesulfonylamino)-phenyl]-acrylic acid

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1016/S0960-894X(01)00552-2

Reference yield:

: 314054-03-0
N-(4-iodo-phenyl)-4-methoxy-benzenesulfonamide

: N-hydroxy-3-[4-(4-methoxy-benzenesulfonylamino)-phenyl]-acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: Pd₂(dba)3; tri-o-tolylphosphine; Et₃N / dimethylformamide / 100 °C

2.1: 1-(3-dimethylaminopropyl)-3-ethyl-carbodiimide hydrochloride; hydroxybenzotriazole hydrate / dimethylformamide / 20 °C

2.2: dimethylformamide / 50 °C

3.1: 10-camphorsulfonic acid / methanol / 20 °C

With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; (1S)-10-camphorsulfonic acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tris-(o-tolyl)phosphine; In methanol; N,N-dimethyl-formamide; 1.1: Heck coupling;
DOI:10.1021/jm020377a