methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

Base Information

Chemical Name:methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate
CAS No.:1132941-14-0
Molecular Formula:C₁₇H₂₂N₂O₅
Molecular Weight:334.372
Hs Code.:

Synonyms:methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

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Technology Process of methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

There total 5 articles about methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1132941-85-5
3-(3-tert-butyl-4-methoxy-5-(methoxycarbonyl)phenylamino)propanoic acid

: 57-13-6
urea

: 1132941-14-0
methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

Guidance literature:: With acetic acid; at 120 ℃; for 18.5h;

Reference yield:

: 15018-03-8
methyl 3,5‐di‐tert-butyl‐2‐hydroxybenzoate

: 1132941-14-0
methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: nitric acid; acetic acid / 2.5 h / 20 °C

2: potassium carbonate / acetone / Reflux

3: iron; ammonium chloride / methanol; water / 1 h / Reflux

4: toluene / 24 h / Reflux

5: acetic acid / 18.5 h / 120 °C

With nitric acid; iron; potassium carbonate; ammonium chloride; acetic acid; In methanol; water; acetic acid; acetone; toluene;
DOI:10.1021/acs.jmedchem.7b01630

Reference yield:

: 372137-83-2
methyl 3-tert-butyl-2-hydroxy-5-nitrobenzoate

: 1132941-14-0
methyl 3-tert-butyl-5-(2,4-dioxotetrahydropyrimidin-1(2H)-yl)-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / Reflux

2: iron; ammonium chloride / methanol; water / 1 h / Reflux

3: toluene / 24 h / Reflux

4: acetic acid / 18.5 h / 120 °C

With iron; potassium carbonate; ammonium chloride; In methanol; water; acetic acid; acetone; toluene;
DOI:10.1021/acs.jmedchem.7b01630