N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

Base Information

Chemical Name:N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine
CAS No.:1262680-53-4
Molecular Formula:C₂₈H₂₉NO₂
Molecular Weight:411.544
Hs Code.:

Synonyms:N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

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Technology Process of N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

There total 1 articles about N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 627-37-2
N-methyl-N-allylamine

: 40167-10-0
2-[4-(benzyloxy)phenyl]acetaldehyde

: 768-60-5
4-methoxyphenylacetylen

: 1262680-53-4
N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

Guidance literature:: With copper(I) bromide; In toluene; at 100 ℃; for 0.416667h; Inert atmosphere; Microwave irradiation;
DOI:10.1002/anie.201004256

Reference yield: 96.0%

: 1262680-53-4
N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

: 1262680-30-7
1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; In dichloromethane; at 40 ℃; Inert atmosphere; Reflux;
DOI:10.1002/anie.201004256

Reference yield:

: 1262680-53-4
N-allyl-1-(4-(benzyloxy)phenyl)-4-(4-methoxyphenyl)-N-methylbut-3-yn-2-amine

: C₃₄H₃₃N₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: Thiosalicylic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 20 °C / Inert atmosphere

2.1: chloro-trimethyl-silane / acetonitrile / 0.17 h / Inert atmosphere

2.2: 1 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; chloro-trimethyl-silane; Thiosalicylic acid; In dichloromethane; acetonitrile;
DOI:10.1021/acs.joc.5b01703