4-chloro-N-(prop-2-yn-1-yl)benzamide

Base Information

Chemical Name:4-chloro-N-(prop-2-yn-1-yl)benzamide
CAS No.:24911-37-3
Molecular Formula:C10H8 Cl N O
Molecular Weight:193.633
Hs Code.:
Mol file:24911-37-3.mol

Synonyms:Benzamide,4-chloro-N-2-propynyl- (9CI); Benzamide, p-chloro-N-2-propynyl- (8CI);4-Chlorophenylcarbamic acid 2-propynyl ester

Suppliers and Price of 4-chloro-N-(prop-2-yn-1-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-(prop-2-yn-1-yl)benzamide

Chemical Property:

Vapor Pressure:5.72E-05mmHg at 25°C
Boiling Point:346.5°C at 760 mmHg
Flash Point:163.4°C
PSA：29.10000
Density:1.221g/cm³
LogP:2.09390

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-chloro-N-(prop-2-yn-1-yl)benzamide

There total 4 articles about 4-chloro-N-(prop-2-yn-1-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 122-01-0
4-chloro-benzoyl chloride

: 2450-71-7
Propargylamine

: 24911-37-3
4-chloro-N-(prop-2-yn-1-yl)benzamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 23 ℃; for 17h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.202101751

Reference yield: 73.0%

: 2450-71-7
Propargylamine

: 74-11-3
para-chlorobenzoic acid

: 24911-37-3
4-chloro-N-(prop-2-yn-1-yl)benzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acsmedchemlett.8b00287

Reference yield: 73.0%

: 24911-37-3
4-chloro-N-(prop-2-yn-1-yl)benzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;