(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

Base Information

Chemical Name:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate
CAS No.:1082984-76-6
Molecular Formula:C₃₁H₃₇O₂P
Molecular Weight:472.607
Hs Code.:

Synonyms:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

Chemical Property:

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Technology Process of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

There total 4 articles about (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75468-42-7
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

: 74-88-4
methyl iodide

: 1082984-76-6
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

Guidance literature:: In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.09.010

Reference yield:

: 16832-20-5,32815-12-6,55284-67-8
(1R,2S,5R)-menthol bromoacetate

: 1082984-76-6
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2.5 h / Inert atmosphere; Reflux

2: sodium hydroxide / water; toluene / 3.08 h / Inert atmosphere

3: sodium hydroxide / water; toluene / 3.08 h / Inert atmosphere

4: dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene; 4: |Wittig Olefination;
DOI:10.1039/c3ob27111k

Reference yield:

: 75468-48-3
(L)-carbomenthyloxymethyl triphenylphosphonium bromide

: 1082984-76-6
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water; toluene / 3.08 h / Inert atmosphere

2: sodium hydroxide / water; toluene / 3.08 h / Inert atmosphere

3: dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium hydroxide; In dichloromethane; water; toluene; 3: |Wittig Olefination;
DOI:10.1039/c3ob27111k