C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

Base Information

Chemical Name:C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾
CAS No.:1613454-85-5
Molecular Formula:C₂₅H₂₄FN₆O
Molecular Weight:442.505
Hs Code.:

C<sub>25</sub>H<sub>24</sub><sup>(18)</sup>FN<sub>6</sub>O<sup>(1+)</sup>

Synonyms:C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

Chemical Property:

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Technology Process of C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

There total 13 articles about C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1314081-20-3
[¹⁸F]6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

: 1613454-85-5
C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

Guidance literature:: With copper(ll) sulfate pentahydrate; In water; dimethyl sulfoxide; Inert atmosphere;
DOI:10.1039/c3ob42379d

Reference yield:

: 51787-75-8
4,4'-dinitro-2-biphenylamine

: 1613454-85-5
C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 12 steps

1: 24 h / Inert atmosphere; Reflux

2: ammonium formate; 20% palladium hydroxide-activated charcoal / methanol; ethyl acetate / 3 h / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 23 °C / Inert atmosphere

4: trichlorophosphate / 6 h / Inert atmosphere; Reflux

5: hydrogen bromide / 72 h / Inert atmosphere; Reflux

6: tert-butyl alcohol / 48 h / 23 °C / Inert atmosphere

7: potassium carbonate / toluene; acetone / 8 h / Inert atmosphere; Reflux

8: tetrahydrofuran / 120 h / Inert atmosphere; Reflux

9: sodium cyanoborohydride / methanol / 3 h / 23 °C / Inert atmosphere

10: trifluoroacetic acid; ascorbic acid / water / 0.25 h / 20 °C / Inert atmosphere

11: sodium L-ascorbate; copper(ll) sulfate pentahydrate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; acetonitrile; water / 0.17 h / 20 °C / Inert atmosphere; Cooling with ice

12: copper(ll) sulfate pentahydrate / water; dimethyl sulfoxide / Inert atmosphere

With copper(ll) sulfate pentahydrate; 20% palladium hydroxide-activated charcoal; hydrogen bromide; ammonium formate; sodium cyanoborohydride; potassium carbonate; sodium L-ascorbate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ascorbic acid; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1039/c3ob42379d

Reference yield:

: 1314081-04-3
di-tert-butyl [6-(4-hydroxyphenyl)phenanthridine-3,8-diyl]dicarbamate

: 1613454-85-5
C₂₅H₂₄⁽¹⁸⁾FN₆O⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / toluene; acetone / 8 h / Inert atmosphere; Reflux

2: tetrahydrofuran / 120 h / Inert atmosphere; Reflux

3: sodium cyanoborohydride / methanol / 3 h / 23 °C / Inert atmosphere

4: trifluoroacetic acid; ascorbic acid / water / 0.25 h / 20 °C / Inert atmosphere

5: sodium L-ascorbate; copper(ll) sulfate pentahydrate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; acetonitrile; water / 0.17 h / 20 °C / Inert atmosphere; Cooling with ice

6: copper(ll) sulfate pentahydrate / water; dimethyl sulfoxide / Inert atmosphere

With copper(ll) sulfate pentahydrate; sodium cyanoborohydride; potassium carbonate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; ascorbic acid; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;
DOI:10.1039/c3ob42379d