methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

Base Information

Chemical Name:methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate
CAS No.:915771-74-3
Molecular Formula:C₂₅H₂₂ClNO₆
Molecular Weight:467.906
Hs Code.:

Synonyms:methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

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Chemical Property of methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

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Technology Process of methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

There total 7 articles about methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915770-55-7
3-chloro-2,4-difluoro-N-(2-hydroxyethyl)-N-methyl-benzamide

: 54915-31-0
methyl 3-(benzyloxy)-5-hydroxybenzoate

: 915771-74-3
methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

: C₂₄H₂₀ClNO₆

Guidance literature:: 3-chloro-2,4-difluoro-N-(2-hydroxyethyl)-N-methyl-benzamide; methyl 3-(benzyloxy)-5-hydroxybenzoate; With caesium carbonate; In acetonitrile; at 160 ℃; for 8h; Microwave;

In water; ethyl acetate; pH=2;

Reference yield:

: 67-56-1
methanol

: C₂₄H₂₀ClNO₆

: 915771-74-3
methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

Guidance literature:: With thionyl chloride; at -35 - 20 ℃; for 19h;

Reference yield:

: 100-39-0
benzyl bromide

: 915771-74-3
methyl 3-[(9-chloro-4-methyl-5-oxo-2,3,4,5-tetrahydro-1,4-benzoxazepin-8-yl)oxy]-5-[(phenylmethyl)oxy]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2.1: caesium carbonate / acetonitrile / 8 h / 160 °C / Microwave

2.2: pH 2

With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; acetonitrile;