(RS)-4-nitro-α-phenylbenzenemethyl acetate

Base Information

Chemical Name:(RS)-4-nitro-α-phenylbenzenemethyl acetate
CAS No.:101402-05-5
Molecular Formula:C₁₅H₁₃NO₄
Molecular Weight:271.273
Hs Code.:

Synonyms:(RS)-4-nitro-α-phenylbenzenemethyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (RS)-4-nitro-α-phenylbenzenemethyl acetate

Chemical Property:

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Technology Process of (RS)-4-nitro-α-phenylbenzenemethyl acetate

There total 4 articles about (RS)-4-nitro-α-phenylbenzenemethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 720-44-5
1-(4-methoxyphenyl)-1-phenylmethanol

: 7515-72-2,33149-65-4,33149-68-7
1-[chlorophenylmethyl]-4-nitrobenzene

: 101402-05-5
(RS)-4-nitro-α-phenylbenzenemethyl acetate

Guidance literature:: With acetyl chloride; In dichloromethane; Yield given; 1.) 0 deg C, 2.) room temperature, 1 h;
DOI:10.1016/S0040-4020(01)80747-X

Reference yield: 82.0%

: 720-44-5
1-(4-methoxyphenyl)-1-phenylmethanol

: 75-36-5
acetyl chloride

: 7515-72-2,33149-65-4,33149-68-7
1-[chlorophenylmethyl]-4-nitrobenzene

: 101402-05-5
(RS)-4-nitro-α-phenylbenzenemethyl acetate

Guidance literature:: In dichloromethane; Yields of byproduct given; 1.) 0 deg C, 2.) room temperature, 1 h;
DOI:10.1016/S0040-4020(01)80747-X

Reference yield:

: 611-94-9
4-Methoxybenzophenone

: 101402-05-5
(RS)-4-nitro-α-phenylbenzenemethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / NaBH₄ / dioxane; H₂O / 24 h / Ambient temperature

2: 82 percent / CH₂Cl₂ / 1.) 0 deg C, 2.) room temperature, 1 h

With sodium tetrahydroborate; In 1,4-dioxane; dichloromethane; water;
DOI:10.1016/S0040-4020(01)80747-X