Technology Process of [1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine
There total 9 articles about [1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran; diethyl ether;
at 25 ℃;
for 96h;
Title compound not separated from byproducts;
DOI:10.1021/jo00385a002
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 97 percent / HCl )g) / 1 h / Heating
2: 98 percent / acetic acid, hydrogen / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr
3: 83.7 percent / lithium aluminum hydride / tetrahydrofuran / 16 h / Heating
4: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH2Cl2 / 2.25 h / -55 °C
5: diethyl ether; tetrahydrofuran / 96 h / 25 °C
With
hydrogenchloride; lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; acetic acid; dimethyl sulfoxide;
platinum(IV) oxide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo00385a002
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99.5 percent / H2, acetic acid / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr
2: 81 percent / lithium aluminum hydride / diethyl ether / 16 h / Heating
3: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH2Cl2 / 2.25 h / -55 °C
4: diethyl ether; tetrahydrofuran / 96 h / 25 °C
With
lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; acetic acid; dimethyl sulfoxide;
platinum(IV) oxide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo00385a002
