[1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

Base Information

Chemical Name:[1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine
CAS No.:107383-97-1
Molecular Formula:C₁₂H₂₁N₃
Molecular Weight:207.319
Hs Code.:

Synonyms:[1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

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Chemical Property of [1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

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Technology Process of [1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

There total 9 articles about [1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 107354-37-0
cis,cis-1,3,5-trisformylcyclohexane

: 74-89-5
methylamine

: 107383-92-6
3,5,12-trimethyl-3,5,12-triazawurtzitane<5.3.1.1.0>decane

: 107383-97-1
[1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

Guidance literature:: In tetrahydrofuran; diethyl ether; at 25 ℃; for 96h; Title compound not separated from byproducts;
DOI:10.1021/jo00385a002

Reference yield:

: 554-95-0
benzene-1,3,5-tricarboxylic acid

: 107383-97-1
[1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / HCl )g) / 1 h / Heating

2: 98 percent / acetic acid, hydrogen / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr

3: 83.7 percent / lithium aluminum hydride / tetrahydrofuran / 16 h / Heating

4: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH₂Cl₂ / 2.25 h / -55 °C

5: diethyl ether; tetrahydrofuran / 96 h / 25 °C

With hydrogenchloride; lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; acetic acid; dimethyl sulfoxide; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo00385a002

Reference yield:

: 4105-92-4
triethyl benzene-1,3,5-tricarboxylate

: 107383-97-1
[1-{3,5-Bis-[(E)-methyliminomethyl]-cyclohexyl}-meth-(E)-ylidene]-methyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 99.5 percent / H₂, acetic acid / platinum oxide / 3.5 h / 25 °C / 1034.3 - 2585.7 Torr

2: 81 percent / lithium aluminum hydride / diethyl ether / 16 h / Heating

3: 70 percent / dimethyl sulfoxide, oxalyl chloride / CH₂Cl₂ / 2.25 h / -55 °C

4: diethyl ether; tetrahydrofuran / 96 h / 25 °C

With lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; acetic acid; dimethyl sulfoxide; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo00385a002