4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

Base Information

Chemical Name:4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde
CAS No.:155141-76-7
Molecular Formula:C₁₄H₉ClF₃NO₃
Molecular Weight:331.679
Hs Code.:

Synonyms:4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

Chemical Property:

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Technology Process of 4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

There total 2 articles about 4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 69045-84-7
2,3-dichloro-5-trifluoromethylpyridine

: 155141-76-7
4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

Guidance literature:: With lithium carbonate; In dimethyl sulfoxide; at 100 ℃; for 24h;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 155141-76-7
4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

Guidance literature:: vanillin; With potassium carbonate; at 20 ℃;

2-halo-3-chloro-5-(trifluorometyl)pyridine; With potassium iodide; at 25 - 110 ℃;
DOI:10.1016/j.bmcl.2020.127113

Reference yield: 23.0%

: 155141-76-7
4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde

: 100-36-7
N,N-diethylethylenediamine

: 4303-29-1
4-thioxo-2-thiazolidinone

: 1264752-16-0
(5Z)-5-[(4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxyphenyl)methylidene]-4-{[2-(diethylamino)ethyl]amino}-1,3-thiazol-2(5H)-one

Guidance literature:: N,N-diethylethylenediamine; 4-thioxo-2-thiazolidinone; In ethanol; at 20 ℃; for 3h; Inert atmosphere;

4-{[3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy}-3-methoxybenzaldehyde; With potassium tert-butylate; In ethanol; for 2h; Reflux;