3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

Base Information

Chemical Name:3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide
CAS No.:1352610-24-2
Molecular Formula:C₂₃H₁₉N₇O
Molecular Weight:409.45
Hs Code.:

Synonyms:3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

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Chemical Property of 3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

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Technology Process of 3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

There total 4 articles about 3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1352610-23-1
3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzonitrile

: 1352610-24-2
3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

Guidance literature:: 3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzonitrile; With dihydrogen peroxide; sodium hydroxide; In ethanol; water; at 60 ℃; for 1h;

With hydrogenchloride; In ethanol; water; pH=7 - 8;

Reference yield:

: 614750-82-2
1-(6-methylpyridin-2-yl)-2-[1,2,4]triazolo-[1,5-a]pyridin-6-yl-ethanone

: 1352610-24-2
3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethyl sulfoxide; hydrogen bromide / 2 h / 60 - 70 °C

2.1: ammonium acetate / tert-butyl methyl ether; methanol / 1.5 h / 20 °C / Inert atmosphere

2.2: pH 8 / Inert atmosphere

3.1: sodium hydroxide; dihydrogen peroxide / ethanol; water / 1 h / 60 °C

3.2: pH 7 - 8

With ammonium acetate; hydrogen bromide; dihydrogen peroxide; dimethyl sulfoxide; sodium hydroxide; In methanol; ethanol; tert-butyl methyl ether; water;

Reference yield:

: 614750-85-5
diphenyl (6-methylpyridin-2-yl)(phenylamino)methylphosphonate

: 1352610-24-2
3-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / isopropyl alcohol; tetrahydrofuran / 20 °C

1.2: 1 h

1.3: pH 7 - 8

2.1: dimethyl sulfoxide; hydrogen bromide / 2 h / 60 - 70 °C

3.1: ammonium acetate / tert-butyl methyl ether; methanol / 1.5 h / 20 °C / Inert atmosphere

3.2: pH 8 / Inert atmosphere

4.1: sodium hydroxide; dihydrogen peroxide / ethanol; water / 1 h / 60 °C

4.2: pH 7 - 8

With ammonium acetate; hydrogen bromide; dihydrogen peroxide; caesium carbonate; dimethyl sulfoxide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; tert-butyl methyl ether; water; isopropyl alcohol;