8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol

Base Information

Chemical Name:8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol
CAS No.:94112-58-0
Molecular Formula:C14H18 O3
Molecular Weight:234.295
Hs Code.:2932999099
DSSTox Substance ID:DTXSID80566391
Wikidata:Q82451984
Mol file:94112-58-0.mol

Synonyms:94112-58-0;8-phenyl-1,4-dioxaspiro[4.5]decan-8-ol;8-Phenyl-1,4-dioxaspiro[4,5]decan-8-ol;SCHEMBL612712;DTXSID80566391;JUTTXLGMDSGZCE-UHFFFAOYSA-N;AKOS015152153;AC-13677;8-Phenyl-1,4-dioxa-spiro[4.5]decan-8-ol;A844815

Suppliers and Price of 8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol 95+%
1g
$ 455.00

Chemenu
8-phenyl-1,4-dioxaspiro[4.5]decan-8-ol 95%
1g
$ 430.00

American Custom Chemicals Corporation
8-PHENYL-1,4-DIOXASPIRO[4,5]DECAN-8-OL 95.00%
100MG
$ 970.20

Total 6 raw suppliers

Chemical Property of 8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Refractive Index:1.579
Boiling Point:384.5°Cat760mmHg
Flash Point:186.4°C
PSA：38.69000
Density:1.2g/cm³
LogP:2.19130
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:234.125594432
Heavy Atom Count:17
Complexity:255

Purity/Quality:

99%, ^*data from raw suppliers

8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2(CCC1(C3=CC=CC=C3)O)OCCO2

Technology Process of 8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol

There total 7 articles about 8-Phenyl-1,4-dioxaspiro[4.5]decan-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 4746-97-8
cyclohexanedione monoethylene ketal

: 108-86-1,52753-63-6
bromobenzene

: 94112-58-0
4-hydroxy-4-phenyl-cyclohexanone ethylene ketal

Guidance literature:: bromobenzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere; Reflux;

cyclohexanedione monoethylene ketal; In tetrahydrofuran; for 0.5h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201507320

Reference yield: 97.0%

: 4746-97-8
cyclohexanedione monoethylene ketal

: 5123-13-7
5,5-dimethyl-2-phenyl-1,3,2-dioxaborinane

: 94112-58-0
4-hydroxy-4-phenyl-cyclohexanone ethylene ketal

Guidance literature:: With di-μ-chloro-bis{2-[3-(2,6-diisopropylphenyl)imidazolin-2-ylidene]-3-(phenylthio)phenyl-κ²C,C'}dipalladium(II); potassium carbonate; In toluene; at 120 ℃; for 18h; Sealed tube; Inert atmosphere;
DOI:10.1080/00397911.2019.1594307

Reference yield: 85.0%

: 4746-97-8
cyclohexanedione monoethylene ketal

: 76-84-6
triphenylmethyl alcohol

: 94112-58-0
4-hydroxy-4-phenyl-cyclohexanone ethylene ketal

Guidance literature:: With potassium phosphate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium tert-butylate; C₆₉H₅₇N₂O₂⁽¹⁺⁾*BF₄^(1-)*H⁽¹⁺⁾; In toluene; at 125 ℃; for 24h; Sealed tube;
DOI:10.1016/j.chempr.2021.02.029