C₁₄H₈F₈Sn

Base Information

Chemical Name:C₁₄H₈F₈Sn
CAS No.:1385181-30-5
Molecular Formula:C₁₄H₈F₈Sn
Molecular Weight:446.915
Hs Code.:

C<sub>14</sub>H<sub>8</sub>F<sub>8</sub>Sn

Synonyms:C₁₄H₈F₈Sn

Suppliers and Price of C₁₄H₈F₈Sn

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₈F₈Sn

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₈F₈Sn

There total 1 articles about C₁₄H₈F₈Sn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1559-88-2
1-bromo-2,3,5,6-tetrafluorobenzene

: 753-73-1
dimethyltin dichloride

: 1385181-30-5
C₁₄H₈F₈Sn

Guidance literature:: With isopropylmagnesium chloride; In diethyl ether; under Ar; soln. of i-PrMgCl in Et2O added to soln. of p-C6F4HBr in Et2O at ambient temp.; stirred for 1 h; solid Me2SnCl2 added; stirred for 2 h; filtered; ppt. washed with hexane; solvent removed from extracts under reduced pressure; crystd. on standing; elem. anal.;
DOI:10.1039/c2dt30924f

Reference yield: 74.0%

: 1385181-30-5
C₁₄H₈F₈Sn

: 1385181-33-8
C₁₂H₂BClF₈

Guidance literature:: With boron trichloride; In hexane; at 120 ℃;
DOI:10.1039/c2dt30924f

Reference yield: 74.0%

: 1385181-30-5
C₁₄H₈F₈Sn

: 10294-34-5
boron trichloride

: 1385181-33-8
C₁₂H₂BClF₈

Guidance literature:: In hexane; byproducts: Me2SnCl2; under Ar; Sn compd. reacted with BCl3 in hexane at 120°C; analogously to D. J. Parks, W. E. Piers, G. P. A. Yap, Organometallics, 1998, 17, 5492; purified by fractional sublimation; elem. anal.;
DOI:10.1039/c2dt30924f