Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

Base Information

Chemical Name:Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide
CAS No.:76503-48-5
Molecular Formula:C₁₇H₁₆N₂O₅
Molecular Weight:328.324
Hs Code.:

Synonyms:Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

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Chemical Property of Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

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Technology Process of Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

There total 4 articles about Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 698-63-5
5-nitrofurane-2-carboxaldehyde

: 76503-48-5
Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / benzene / 0.5 h / Ambient temperature

2: 70 percent / aq. NaBH₄, aq.HCl / tetrahydrofuran; aq. ethanol / 1.5 h / -35 °C

3: pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1246/bcsj.56.1107

Reference yield:

: 13060-78-1
2-hydroxy-N-(5-nitrofurfurylidene)aniline

: 76503-48-5
Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / aq. NaBH₄, aq.HCl / tetrahydrofuran; aq. ethanol / 1.5 h / -35 °C

2: pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1246/bcsj.56.1107

Reference yield:

: 95-55-6
2-amino-phenol

: 76503-48-5
Cyclopent-1-enecarboxylic acid (2-hydroxy-phenyl)-(5-nitro-furan-2-ylmethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / benzene / 0.5 h / Ambient temperature

2: 70 percent / aq. NaBH₄, aq.HCl / tetrahydrofuran; aq. ethanol / 1.5 h / -35 °C

3: pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1246/bcsj.56.1107