5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

Base Information

Chemical Name:5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate
CAS No.:910229-66-2
Molecular Formula:C₂₀H₂₈N₂O₄S
Molecular Weight:392.519
Hs Code.:

Synonyms:5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

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Technology Process of 5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

There total 1 articles about 5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5754-18-7
4-methyl-1,2-dihydropyridazine-3,6-dione

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 2,4,6-triisopropyl-benzenesulfonic acid 4-methyl-6-oxo-1,6-dihydro-pyridazin-3-yl ester

: 910229-66-2
5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

Guidance literature:: With pyridine; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2006.06.056

Reference yield: 72.0%

: 910229-66-2
5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

: 1679-18-1
4-Chlorophenylboronic acid

: 32193-12-7
methyl-4 (p-chloro phenyl)-6 pyridazone-3

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 155 ℃;
DOI:10.1016/j.tetlet.2006.06.056

Reference yield: 63.0%

: 910229-66-2
5-methyl-6-oxo-1,6-dihydropyridazin-3-yl 2,4,6-triisopropylbenzenesulfonate

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 118270-06-7
6-(3-Methoxy-phenyl)-4-methyl-2H-pyridazin-3-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 155 ℃;
DOI:10.1016/j.tetlet.2006.06.056