formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

Base Information

Chemical Name:formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle
CAS No.:118975-44-3
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

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Chemical Property of formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

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Technology Process of formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

There total 3 articles about formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 118975-43-2
formyl-3-dihydroxy-3,5-methoxy-4-methyl-6-benzoate de methyle

: 75-26-3
isopropyl bromide

: 118975-44-3
formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 14h;
DOI:10.1002/hlca.19880710424

Reference yield:

: 55366-04-6
hydroxy-3-dimethoxy-4,6-methyl-2-benzoate de methyle

: 118975-44-3
formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / BCl₃ / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) CF₃COOH; 2.) H₂O / 1.) 16 h, 95 deg C; 2.) 5 h, 60 deg C

3: 96 percent / K₂CO₃ / dimethylformamide / 14 h / 40 °C

With water; boron trichloride; potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710424

Reference yield:

: 91062-17-8
dihydroxy-3,6-methoxy-4-methyl-2-benzoate de methyle

: 118975-44-3
formyl-3-diisopropoxy-2,5-methoxy-4-methyl-6-benzoate de methyle

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CF₃COOH; 2.) H₂O / 1.) 16 h, 95 deg C; 2.) 5 h, 60 deg C

2: 96 percent / K₂CO₃ / dimethylformamide / 14 h / 40 °C

With water; potassium carbonate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710424