o-bromobenzyloxypentamethyldisilane

Base Information

• Chemical Name: o-bromobenzyloxypentamethyldisilane
• CAS No.: 201050-10-4
• Molecular Formula: C₁₂H₂₁BrOSi₂
• Molecular Weight: 317.373
• Mol file: 201050-10-4.mol

Synonyms:o-bromobenzyloxypentamethyldisilane

Chemical Property of o-bromobenzyloxypentamethyldisilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-bromobenzyloxypentamethyldisilane

There total 1 articles about o-bromobenzyloxypentamethyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

pentamethylchlorodisilane (1560-28-7) + o-bromobenzyl alcohol (18982-54-2) → o-bromobenzyloxypentamethyldisilane (201050-10-4)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 2h;

DOI:10.1139/v99-250

Reference yield: 84.0%

o-bromobenzyloxypentamethyldisilane (201050-10-4) → o-pentamethyldisilylbenzyl alcohol (201050-04-6)

Guidance literature:

With lithium; In diethyl ether; for 2.5h;

DOI:10.1139/v99-250

Reference yield:

cyclohexenone (930-68-7) + o-bromobenzyloxypentamethyldisilane (201050-10-4) → 3-trimethylsilylcyclohexan-1-one (7531-60-4) + 1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole (321903-29-1)

Guidance literature:

o-bromobenzyloxypentamethyldisilane; With lithium; In diethyl ether; for 2h;

In diethyl ether; for 0.833333h;

cyclohexenone; In diethyl ether; at -80 - 20 ℃; for 21h;

DOI:10.1139/v99-250

upstream raw materials:

pentamethylchlorodisilane

o-bromobenzyl alcohol

Downstream raw materials:

3-trimethylsilylcyclohexan-1-one

1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole

o-pentamethyldisilylbenzyl alcohol