3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

Base Information

Chemical Name:3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane
CAS No.:74789-86-9
Molecular Formula:C₁₀H₁₈BBrO
Molecular Weight:244.967
Hs Code.:

Synonyms:3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

Suppliers and Price of 3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

There total 1 articles about 3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 38673-97-1
1-boraadamantane

: 74789-86-9
3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

: 636-70-4
triethylamine hydrobromide

Guidance literature:: With methanol; bromine; triethylamine; In benzene; (dry Ar); stirred 1 h at 5°C; heated for 5 min at 60°C; cooled; added Et3N and MeOH in 30 min at 20°C; stirred 30 min; solvent distd.; residue treated isopentane; ppt. Et3N*HBr filtered; filtrat distn.; elem. anal.;
DOI:10.1007/BF00949692

Reference yield: 84.0%

: 74789-86-9
3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

: 124-41-4
sodium methylate

: 74789-87-0
C₈H₁₃(CH₂OCH₃)B(OCH₃)

: 7647-15-6
sodium bromide

Guidance literature:: In methanol; (dry Ar); heated for 1.5 h at 50°C; MeOH vac. distd.; residue treated isopentane; ppt. NaBr filtered; filtrate distn.; elem. anal.;
DOI:10.1007/BF00949692

Reference yield: 42.0%

: 74789-86-9
3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

: 109-89-7
diethylamine

: 39238-98-7
3-methoxy-7-methylene-3-borabicyclo{3.3.1.}nonane

: 74789-87-0
C₈H₁₃(CH₂OCH₃)B(OCH₃)

: 74789-89-2
3-methoxy-7-diethylaminomethyl-3-borabicyclo[3.3.1]nonane*HCl

: 6274-12-0
diethylamine hydrobromide

Guidance literature:: With hydrogenchloride; In diethylamine; (dry Ar); heated in sealed ampul for 80 h at 100°C; ppt. Et2NH*HBr filtered; filtrate treated MeOH; fraction vac. distn.; treated ether soln. HCl; sepd.; filtrate distn.; elem. anal.;
DOI:10.1007/BF00949692