O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

Base Information

Chemical Name:O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate
CAS No.:866927-59-5
Molecular Formula:C₁₅H₂₃O₆P
Molecular Weight:330.318
Hs Code.:

Synonyms:O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

Suppliers and Price of O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

There total 2 articles about O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 762-04-9
phosphonic acid diethyl ester

: 53936-56-4
4-(tetrahydro-2H-2-pyranyloxy)phenol

: 866927-59-5
O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

Guidance literature:: With triethylamine; In tetrachloromethane;
DOI:10.1016/j.jorganchem.2005.05.023

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 866927-59-5
O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃

2: 88 percent / NEt₃ / CCl₄

With aluminium trichloride; triethylamine; In tetrachloromethane;
DOI:10.1016/j.jorganchem.2005.05.023

Reference yield: 82.0%

: 866927-59-5
O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate

: 1066-45-1
trimethyltin(IV)chloride

: 7440-23-5
sodium

: 108613-04-3
trimethyl(4-tetrahydro-2H-2-pyranyloxyphenyl)stannane

Guidance literature:: In ammonia; Irradiation (UV/VIS); under inert atm.; into flask cooled with acetone-liq. N2 was condensed NH3; Me3SnCl dissolved; Na added; O,O-diethyl O-4-tetrahydro-2H-2-pyranyloxyphenyl phosphate added; soln. irradiated with stirring for 4 h; quenched by adding NH4Cl in excess; NH3 allowed to evap.; residue treated (H2O); extd. (Et2O); extracts washed (brine); dried (MgSO4); solvent removed; as oil;
DOI:10.1016/j.jorganchem.2005.05.023