(E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester

Base Information

• Chemical Name: (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester
• CAS No.: 50906-19-9
• Molecular Formula: C₁₃H₁₅BrO₄
• Molecular Weight: 315.164
• Mol file: 50906-19-9.mol

Synonyms:(E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester

Chemical Property of (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester

There total 4 articles about (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.1%

→ (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester (50906-19-9)

Guidance literature:

With potassium carbonate; In acetone; for 0.25h;

In acetone; at 55 ℃;

Reference yield:

methyl ferulate (22329-76-6,34298-89-0,2309-07-1) + ethylene dibromide (106-93-4) → (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester (50906-19-9)

Guidance literature:

methyl ferulate; With potassium carbonate; In acetone; for 0.25h;

ethylene dibromide; Reflux; Darkness;

DOI:10.2174/1573406411309060012

Reference yield:

ethyl bromide (74-96-4) + methyl ferulate (22329-76-6,34298-89-0,2309-07-1) → (E)-3-[4-(2-Bromo-ethoxy)-3-methoxy-phenyl]-acrylic acid methyl ester (50906-19-9)

Guidance literature:

With potassium carbonate; In acetone; at 50 ℃;

DOI:10.1016/j.ejmech.2019.04.050

upstream raw materials:

methyl ferulate

ethylene dibromide

3-(4-hydroxy-3-methoxyphenyl)acrylic acid

ethyl bromide